SYNCHROTRON BASED X-RAY ABSORPTION SPECTROS-COPY FOR STRUCTURAL ANALYSIS OF BASALT FIBERS

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dc.contributor.authorLichtenberg, Henning
dc.contributor.authorMahltig, Boris
dc.contributor.authorKlysubun, Wantana
dc.contributor.authorPrange, Alexander
dc.contributor.authorHormes, Josef
dc.contributor.organizationTechnická univerzita v Liberci
dc.date.accessioned2024-10-01T09:40:44Z
dc.date.available2024-10-01T09:40:44Z
dc.description.abstractX-ray Absorption Near Edge Structure (XANES) spectroscopy at the Synchrotron Light Research Institute (Thailand) was used to investigate temperature related structural changes in basalt fibers. As a first step, XANES spectra of fiber samples cut from a basalt roving heated for 1 hour at 800 °C were recorded at the K absorption edges of three chemical elements and compared with the spectra of the untreated fibers. Silicon and calcium K-edge XANES spectra of the fibers were not affected by heating, whereas iron K-edge XANES spectra were significantly influenced by heating at 800 °C. The high iron content in basalt fibers has been attributed to their higher thermal stability compared to common natural or synthetic fibers. As a next step, iron K-edge XANES spectra of two types of fibers (basalt roving and uncoated chopped fibers) were recorded after heating at temperatures between 600 °C and 900 °C. In both cases, with increasing temperature the absorption edge shifts to higher energies, indicating progressing oxidation of the iron atoms in the fibers. These experiments demonstrate the potential of X-ray absorption spectroscopy as a powerful analytical tool to investigate structural changes in basalt fibers upon heating and to correlate them with changes in their mechanical properties.cs
dc.formattext
dc.format.extent10 stran
dc.identifier.doi10.15240/tul/008/2024-2-008
dc.identifier.issn1335-0617
dc.identifier.urihttps://dspace.tul.cz/handle/15240/175351
dc.language.isocscs
dc.publisherTechnical University of Liberec
dc.publisher.abbreviationTUL
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dc.relation.ispartofFibres and Textiles
dc.subjectCompression stockingcs
dc.subject4D body scanningcs
dc.subjectLower legcs
dc.subjectBody size and shapecs
dc.subjectDynamic positioncs
dc.titleSYNCHROTRON BASED X-RAY ABSORPTION SPECTROS-COPY FOR STRUCTURAL ANALYSIS OF BASALT FIBERSen
dc.typeArticleen
local.accessopen access
local.citation.epage65
local.citation.spage56
local.facultyFaculty of Textile Engineeringen
local.fulltextyesen
local.relation.issue2
local.relation.volume31
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