Ag-AgCl Nanoparticles Fixation on Electrospun PVA Fibres: Technological Concept and Progress

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dc.contributor.authorVilamová, Zuzana
dc.contributor.authorKonvičková, Zuzana
dc.contributor.authorMikeš, Petr
dc.contributor.authorHolišová, Veronika
dc.contributor.authorMančík, Pavel
dc.contributor.authorDobročka, Edmund
dc.contributor.authorKratošová, Gabriela
dc.contributor.authorSeidlerová, Jana
dc.date.accessioned2019-11-12T09:48:41Z
dc.date.available2019-11-12T09:48:41Z
dc.date.issued2019-12
dc.description.abstractPolymer-metal based material with unique 3D structure is an attractive substrate for the development of biomedical applications. A novel preparation of the composite from polymer fibres and silver nanoparticles has been designed through: (1) preparation of silver nanoparticles by phytosynthesis and (2) incorporation of these nanoparticles in a fibrous membrane prepared by electrospinning. The nanoparticle biosynthesis was performed in a pure environmental-friendly, easy, static, bottom-up in vitro regime using Tilia sp. leachate. TEM and XRD depict the formation, stabilisation and encapsulation of crystalline silver (14 ± 9 nm) nanoparticles (NPs) in one simple step with low tendency to aggregate. We achieved successful incorporation in the uniform electrospun 221 ± 24 nm poly(vinylalcohol) fibres, and this confirms the possibility of its use in the biomedical field. Both SEM with EDX and TEM analysis determined fibre uniformity with the presence of silver NPs, and ICP-AES confirmed the relatively similar metal concentration throughout the triplicate measurement of fibre structures on the 2 × 2 cm area in the following manner: 0.303 ± 0.018 wt. %, 0.282 ± 0.017 wt. %, and 0.281 ± 0.017 wt. %. Our hypothesis is based on previously verified preparation of active silver NPs and the easily prepared PVA electrospun fibres which act as a water soluble matrix. The simple methodology of incorporating biosynthetically prepared NPs in the PVA fibers highlights the effectiveness of this material, with simple release from water-soluble PVA and final activation of the prepared NPs.cs
dc.format.extent10 strancs
dc.identifier.doi10.1038/s41598-019-51642-7
dc.identifier.urihttps://dspace.tul.cz/handle/15240/154103
dc.identifier.urihttps://www.nature.com/articles/s41598-019-51642-7
dc.language.isocscs
dc.publisherNature Publishing Group
dc.relation.ispartofScientific Reports
dc.titleAg-AgCl Nanoparticles Fixation on Electrospun PVA Fibres: Technological Concept and Progresscs
local.accessopen access
local.article.number15520
local.relation.issue1
local.relation.volume9
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